Apostolos Spyros, Assoc. Prof.

Publications*

70	"Olive fruit phenolic profiling using High Resolution-Magic Angle Spinning (HR-MAS) solid state NMR spectroscopy". E. Manolopoulou, A. Spyros, in Metabolic Profiling: Methods and Protocols, Methods in Molecular Biology, 2nd Edition, G. A. Theodoridis, H. Gika, O. Deda, I. Wilson (Eds), Springer-Nature, 2024, in press.
69	"1H NMR based sulfonation reaction kinetics of wine relevant thiols in comparison with known carbonyls". S. Tachtalidou, A. Spyros, N. Sok, S.S. Heinzmann, F. Denate, P. Schmit-Kopplin, R.D. Gougeon, M. Nikolantonaki Food Chem., 2024, in press. (link).
68	"A study of Greek graviera cheese by NMR-based metabolomics". E. Ralli and A. Spyros Molecules, 2023, 28, 5488. (link).
67	"Fabrication of 3D-printed octreotide acetate-loaded oral solid dosage forms by means of semi-solid extrusion printing". A.-T. Chatzitaki, G. Eleftheriadis, K. Tsongas, D. Tzetzis, A. Spyros, I.S.Vizirianakis, D.G. Fatouros Int. J. Pharm., 2023, 632, 122569. (link).
66	"Structural and physicochemical characterization of an aminosugar-rich exopolysaccharide isolated from a Chlorella sp". E. Kokarakis, T. Nazos, L. Mavroudakis, N.-C. Stratigakis, G. Sfendourakis, S. Lioudaki, A. Spyros, S. Pergantis, D. Ghanotakis Algal Res., 2022, 68, 102881. (link).
65	"Optimisation of the HS-SPME/GC-MS approach by design of experiments combined with chemometrics for the classification of Cretan virgin olive oils". A. Lioupi, I. Sampsonidis, C. Virgiliou, V.T. Papoti, K.G. Zinoviadou, A. Spyros and G. Theodoridis, Metabolites, 2022, 12, 114. (link).
64	"Effects of deficit irrigation on 'Koroneiki' olive tree growth, physiology and olive oil quality at different harvest dates". M. Siakou, A. Bruggeman, M. Eliades, C. Zoumides, H. Djuma, M.C. Kyriacou, M. G. Emmanouilidou, A. Spyros, E. Manolopoulou, A. Moriana, Agric. Wat. Manag., 2021, 258, 107200. (link).
63	"Polyhydroxyalkanoate (PHA) production in Pseudomonas sp. phDV1 strain grown on phenol as carbon sources". I. Kanavaki, A. Drakonaki, E.D. Geladas, A. Spyros, H. Xie, G. Tsiotis, Microorganisms, 2021, 9, 1636. (link).
62	"FoodOmicsGR_RI: a consortium for comprehensive molecular characterisation of food products". G. Theodoridis, A. Pechlivanis, N. S. Thomaidis, A. Spyros, C. A. Georgiou, T. Albanis, I. Skoufos, S. Kalogiannis, G. Th. Tsangaris, A. S. Stasinakis, I. Konstantinou, A. Triantafyllidis, K. Gkagkavouzis, A. S. Kritikou, M. E. Dasenaki, H. Gika, C. Virgiliou, D. Kodra, N. Nenadis, I. Sampsonidis, G. Arsenos, M. Halabalaki, E. Mikros, Metabolites, 2021, 11, 74. (link).
61	"Enantioselective synthesis of a costic acid analogue with acaricidal activity against the bee parasite Varroa destructor". S. Georgiladaki , D. Isaakidis , A. Spyros , G. K. Tsikalas and H. E. Katerinopoulos, R. Soc. Open Sci., 2020, 7, 200612.
60	"Nuclear Magnetic Resonance". J. Janovick, A. Spyros, P. Dais and E. Hatzakis, in Chemical Analysis of Food (Second Edition), Y. Pico (Ed.), Academic Press, Elsevier Inc., 2020, pp. 135-175. (Book chapter)
59	"Near-equal compressibility of liver oil and seawater minimises buoyancy changes in deep-sea sharks and chimaeras". I. G. Priede, R. W. Burgass, M. Mandalakis, A. Spyros, P. Gikas, F. Burns and J. Drewery, J. Exp. Biol., 2020, 223, jeb22294.
58	"Magnetic resonance applications in food analysis". F. Tang, M. Vasas, E. Hatzakis and A. Spyros, Annu. Rep. NMR Spectrosc., 2019, 98, 239.
57	"Significant metabolic improvement by a water extract of olives: animal and human evidence". N. Peroulis, V. P. Androutsopoulos, G. Notas, S. Koinaki, E. Giakoumaki, A. Spyros, E. Manolopoulou, S. Kargaki, M. Tzardi, E. Moustou, E. G. Stephanou, E. Bakogeorgou, N. Malliaraki, M. Niniraki, C. Lionis, E. Castanas, and M. Kampa, Europ. J. Nutr., 2019, 58, 2545.
56	"NMR Spectroscopy". A. Spyros, in Fingerprinting Techniques in Food Authentication and Traceability, KS. Siddiqi, L. Nollet (Eds), CRC Press, Boca Raton, Florida, USA, 2018, Ch. 3, 45.
55	"NMR spectroscopy protocols for food metabolomics applications". E. Ralli, M. Amargianitaki, E. Manolopoulou, M. Misiak, G. Markakis, S. Tachtalidou, A. Kolesnikova, P. Dais and A. Spyros, in Metabolic Profiling: Methods and Protocols, Methods in Molecular Biology, vol. 1738, G. A. Theodoridis, H. Gika, I. Wilson (Eds), Humana Press, New York, NY, 2018, Ch. 14, 203. (link).
54	"NMR-based metabolomics in wine quality control and authentication". M. Amargianitaki and A. Spyros, Chem. Biol. Technol. Agric., 2017, 4:9. (link, pdf).
53	"Phosphorus derivatization as a tool to enhance specificity of quantitative NMR analysis of foods". A. Spyros, Modern Magnetic Resonance, 2nd Edition, G. Webb (Ed), Springer International Publishing, Netherlands, 2017. (link).
52	"Use of costic acid, a natural extract from Dittrichia viscosa, for the control of Varroa destructor, a parasite of the European honey bee". K. Sofou, D. Isaakidis, A. Spyros, A. Buttner, A. Giannis and H. E. Katerinopoulos, Beilstein J. Org. Chem., 2017, 13, 952. (link, pdf).
51	"Liquid-state NMR in cultural heritage and archaeological sciences". A. Spyros, Modern Magnetic Resonance, 2nd Edition, G. Webb (Ed), Springer International Publishing, Netherlands, 2016. (link).
50	"Application of NMR in food analysis". A. Spyros, SPR Nuclear Magnetic Resonance vol. 45, V. Ramesh (Ed), Royal Society of Chemistry, Cambridge, UK, 2016, Chapt. 9. (Book chapter).
49	" Identification and quantification of aromatic hydrocarbons adsorbed on soot from premixed flames of kerosene, synthetic kerosene, and kerosene-synthetic biofuels". A. Andrade-Eiroa, R. Shahla, M. Romanias, P. Dagaut, E. Karafas, A. Spyros, and G. Dayma, Energy & Fuels, 2015, 29, 6556.
48	"Identification and quantitative determination of carbohydrate molecules in Greek honey by employing 13C NMR spectroscopy". A. Kazalaki, M. Misiak, A. Spyros and P. Dais, Anal. Methods, 2015, 7, 5962.
47	"Investigation of the photochemical reactivity of soot particles derived from biofuels toward NO2. A kinetic and product study". M. Romanias, P. Dagaut, Y. Bedjanian, A. Andrade-Eiroa, R. Shahla, E. Karafas, V.P. Papadimitriou, and A. Spyros, J. Phys. Chem. A, 2015, 119, 2006.
46	"Egg yolk identification and aging in mixed paint binding media by NMR spectroscopy". S. Sfakianaki, E. Kouloumpi, D. Anglos, A. Spyros, Magn. Reson. Chem., 2015, 53, 22.
45	"Nuclear Magnetic Resonance". A. Spyros, in Handbook of Food Analysis (3rd Ed.), L. Nollet, F. Todra (Eds), CRC Press, Boca Raton, Florida, USA, 2015, Ch. 35, 659. (Book chapter)
44	"Heptanuclear lanthanide [Ln7] clusters: from blue-emitting solution-stable complexes to hybrid clusters". A. Canaj, G. Tsikalas, A. Philippidis, A. Spyros and C. Milios, Dalton Trans., 2014, 43, 12486. (link)
43	"NMR spectroscopy analysis of polyester resins as contemporary art materials". A. Spyros, U. Knuutinen in Impact of the Indoor Environment on the Preservation of our Moveable Heritage, Havermans, J., Adriaens, M., Thickett, D., Strlic, M., Fassina, V. and Rabin, I. (Eds), Nardini Editore, 2014, in press. (Book chapter)
42	"Carbon-dot organic surface modifier analysis by solution-state NMR spectroscopy". A. Fillipidis, A. Spyros, D. Anglos, A. Bourlinos, R. Zboril, E. P. Giannelis, J. Nanopart. Res., 2013, 15, 1777. (pdf)
41	"High resolution-magic angle spinning NMR study of olive leaves". E. Manolopoulou, A. Spinella, E. Caponetti, P. Dais and A. Spyros in Magnetic Resonance in Food Science: Food for Thought, J. van Duynhoven (Ed), Royal Society of Chemistry, Cambridge, UK, 2013, pp. 164-170. (Book chapter)
40	"NMR spectroscopy in food analysis". A. Spyros, P. Dais, Royal Society of Chemistry, Cambridge, UK, 2013, pp. 1-329. (Monograph)
39	"Nuclear Magnetic Resonance". A. Spyros, P. Dais, in Chemical Analysis of Food: Techniques and Applications, Y. Pico (Ed.), Elsevier, Amsterdam, 2012, pp. 91-115. (Book chapter)
38	"Primary and secondary marine organic aerosols over the North Atlantic ocean during the MAP experiment". S. Decesari, E. Finessi, M. Rinaldi, M. Paglione, S. Fuzzi, E. G. Stephanou, T. Tziaras, A. Spyros, D. Ceburnis, C. O'Dowd, M. Dall'Osto, R. M. Harrison, J. Allan, H. Coe, M. C. Facchini, J. Geophys. Res.-Atmosph., 2011, 116, D22210. (pdf)
37	"The adsorption of organophosphates into microporous and mesoporous NaX zeolites and subsequent chemistry". Q. Meng, D. Doetschman, A. Rizos, M.-H. Lee, J. Schulte, A. Spyros, C. Kanyi, Env. Sci. Technol., 2011, 45, 3000. (pdf)
36	"Analysis and aging of unsaturated polyester resins in contemporary art installations by NMR spectroscopy". G. Stamatakis, U. Knuutinen, K. Laitinen, A. Spyros, Anal. Bioanal. Chem., 2010, 398, 3203. , (pdf)
35	"31P NMR spectroscopy in food analysis". A. Spyros, P. Dais, Progr. NMR Spectrosc., 2009, 54, 195. (doi), (pdf) Since publication featured as the 10th, 2nd and 5th most downloaded article in PNMRS.
34	"Geographical characterization of Greek virgin olive oils (Cv. Koroneiki) using 1H and 31P NMR fingerprinting with canonical discriminant analysis and classification binary trees". P. Petrakis, A. Agiomyrgianaki, S. Christophoridou, A. Spyros, P. Dais, J. Agric. Food Chem., 2008, 56, 3200.(pdf)
33	"The isoenzyme seven of tobacco NAD(H)-dependent glutamate dehydrogenase exhibits high deaminating and low aminating activities in vivo". D. S. Skopelitis, N. V. Paranychianakis, A. Kouvarakis, A. Spyros, E. G. Stephanou, and K. A. Roubelakis-Angelakis, Plant. Physiol., 2007, 145, 1726. (pdf)
32	"31P NMR spectroscopy in the quality control and authentication of extra-virgin olive oil: A review of recent progress". P. Dais and A. Spyros, Magn. Reson. Chem., 2007, 45, 367. (pdf) NMR Ezine feature.
31	"Comparison of analytical methodologies based on 1H and 31P NMR spectroscopy with conventional methods of analysis for the determination of some olive oil constituents". P. Dais, A. Spyros, S. Christophoridou, E. Hatzakis, G. Fragaki, A. Agiomyrgianaki, E. Salivaras, G. Siragakis, D. Daskalaki, M. Tasioula-Margari, M. Brenes, J. Agric. Food Chem., 2007, 55, 577.(pdf)
30	"Dynamic light scattering vs 1H NMR investigation of pH-responsive diblock copolymers in water". M. Vamvakaki, D. Palioura, A. Spyros, S. P. Armes, and S. H. Anastasiadis, Macromolecules, 2006, 39, 5106.(pdf)
29	"Studies of organic paint binders by NMR spectroscopy". A. Spyros, D. Anglos, Appl. Phys. A, 2006, 83, 705.(pdf)
28	"Detection of extra virgin olive oil adulteration with lampante olive oil and refined olive oil using NMR spectroscopy and multivariate statistical analysis". G. Fragaki, A. Spyros, G. Siragakis, E. Salivaras, P. Dais, J. Agric. Food. Chem., 2005, 53, 2810.(pdf)
27	"Structure determination of oligomeric alkannin and shikonin derivatives". A. Spyros, A. N. Assimopoulou, V. P. Papageorgiou, Biomed. Chrom., 2005, 19, 498.(pdf)
26	"Correction of the structure of a new sesquiterpene from Cistus creticus ssp. creticus". K. Hatzellis, G. Pagona, A. Spyros, C. Demetzos, H. E. Katerinopoulos, J. Nat. Prod., 2004, 67, 1996.(pdf)
25	"Study of aging in oil paintings by 1D and 2D NMR Spectroscopy". A. Spyros, D. Anglos, Anal. Chem., 2004, 76, 4929.(pdf) feature article.
24	"Kinetics of diglyceride formation and isomerization in virgin olive oils by employing 31P NMR spectroscopy. Formulation of a quantitative measure to assess olive oil storage history". A. Spyros, A. Fillipidis and P. Dais, J. Agric. Food Chem., 2004, 52, 157. (pdf)
23	"Classification of edible oils by employing 31P and 1H NMR Spectroscopy in combination with multivariate statistical analysis. A proposal for the detection of seed oil adulteration in virgin olive oils ". G. Vigli, A. Fillipidis, A. Spyros and P. Dais, J. Agric. Food Chem., 2003, 51, 5715. (pdf)
22	"Characterization of unsaturated polyester and alkyd resins using One and Two-Dimensional NMR spectroscopy". A. Spyros, J. Appl. Polym. Sci., 2003, 88, 1881. (pdf)
21	"The use of L-lysine fluorescence derivatives as tracers enhance the performance of polarization fluoroimmunoassays. A study using the herbicides 2,4D and 2,4,5T as model antigens". G. I. Hatzidakis, S. A. Eremin, E. K. Krambovitis, A. Spyros and A. M. Tsatsakis, Anal. Chem., 2002, 74, 2513. (pdf)
20	"Determination of the diglycerides content in Greek virgin olive oils and some commercial olive oils by employing 31P NMR spectroscopy". P. Fronimaki, A. Spyros, S. Christoforidou and P.Dais, J. Agric. Food Chem., 2002, 50, 2207. (pdf)
19	"Quantitative determination of the distribution of free hydroxylic and carboxylic groups in unsaturated polyester and alkyd resins by 31P NMR spectroscopy". A. Spyros, J. Appl. Polym. Sci., 2002, 83, 1635. (pdf)
18	"31P Nuclear Magnetic Resonance spectroscopy of polyphenol-containing olive oil model compounds". S. Christoforidou, A. Spyros and Photis Dais, Phosphorus Sulfur and Silicon, 2001, 170, 139. (pdf)
17	"Application of 31P-NMR spectroscopy in food analysis. I. Quantitative determination of mono- and diglycerides in virgin olive oils". A. Spyros, Photis Dais, J. Agric. Food Chem., 2000, 48, 802 . (pdf)
16	"NMR study of the rotational dynamics of linear homopolysaccharides in dilute solutions as a function of linkage position and stereochemistry". E. Tylianakis, A. Spyros, Photis Dais, F. Taravel, and A. Perico, Carbohydr. Res., 1999, 315, 16. (pdf)
15	"CYCLCROP mapping of 13C labelled compounds: Perspectives in polymer science and plant physiology". M. Heidenreich, A. Spyros, W. K?ckenberger, N. Chandrakumar, R. Bowtell and R. Kimmich, in Spatially Resolved Magnetic Resonance,Blumler, P. Blumich, B. Botto, R. Fukushima E. (Eds), Wiley-VCH, Weinheim, 1998. (Book chapter)
14	"Selective determination of elastomer distribution in multicomponent systems using proton-detected 13C imaging". A. Spyros, N. Chandrakumar, M. Heidenreich and R. Kimmich, Macromolecules 1998, 31, 3021. (pdf)
13	"1H NMR imaging study of enzymatic degradation in poly(3-hydroxybutyrate) and poly(3-hydroxybutyrate-co-3-hydroxyvalerate). Evidence for preferential degradation of the amorphous phase by PHB depolymerase B from Pseudomonas lemoignei". A. Spyros, R. Kimmich, B. H. Briese and D. Jendrossek, Macromolecules 1997, 30, 8218. (pdf)
12	"A study of polyhydroxyalkanoates by quantitative 31P NMR Spectroscopy: Molecular weight and chain cleavage". A. Spyros, D. S. Argyropoulos, and R. H. Marchessault, Macromolecules 1997, 30, 327. (pdf)
11	"13C and 1H amorphous linewidths in semicrystalline poly(4-hydroxybutyrate) and poly(3-hydroxybutyrate-co-4-hydroxybutyrate) above Tg by high resolution and solid state NMR experiments". A. Spyros and R. H. Marchessault, J. Polym. Sci. Part B: Polym. Phys. 1996, 34, 1777.(pdf)
10	"Segmental dynamics in poly(3-hydroxybutyrate-co-4-hydroxybutyrate)s above Tg: 13C Nuclear Magnetic Relaxation in the amorphous phase". A. Spyros and R. H. Marchessault, Macromolecules, 1996, 29, 2479. (pdf)
9	"13C Nuclear Magnetic Relaxation measurements of poly(4-hydroxybutyrate) and poly(3-hydroxybutyrate-co-4-hydroxybutyrate) in the bulk". A. Spyros, R. H. Marchessault, Macromolecules, 1995, 28, 6108. (pdf)
8	"13C Nuclear Magnetic Relaxation and local dynamics of synthetic polymers in solution and in the bulk". P. Dais and A. Spyros, Progr. NMR Spectrosc. 1995, 27, 555. (pdf)
7	"Local chain motions of poly(beta-hydroxyoctanoate) in the bulk. 13C NMR relaxation study". A. Spyros, P. Dais and R.H. Marchessault, J. Polym. Sci. Polym. Phys. Ed. 1995, 33, 366. (abstract)
6	"Composite spectral density functions for the interpretation of the 13C NMR relaxation behaviour of polymers containing hydrocarbon side chains. Free and restricted side chain motion". A. Spyros and P. Dais, J. Polym. Sci. Polym. Phys. Ed. 1995, 33, 353. (abstract)
5	"Viscosity dependence of chain segmental motion and side chain internal rotation of poly(1-naphthylmethyl acrylate) in dilute solution. Carbon-13 Nuclear Magnetic Relaxation study". A. Spyros, P. Dais and F. Heatley, Macromolecules, 1994, 27, 6207. (pdf)
4	"Chain segmental motion and sidechain internal rotations of poly(1-naphthylalkyl acrylate)s in solution studied by 13C Nuclear Magnetic Relaxation". A. Spyros, P. Dais and F. Heatley, Macromolecules, 1994, 27, 5845. (pdf)
3	"Assignment of the 1H and 13C NMR spectra and stereochemical analysis of radical-initiated poly(1- naphthylmethyl acrylate) and poly(2-(1-naphthyl)ethyl acrylate)". A. Spyros, P. Dais and F. Heatley, Macromol. Chem. Phys. 1994, 195, 3271.
2	"Microstructure determination of poly(1-naphthylalkyl methacrylate)s by 13C NMR spectroscopy". T. Radiotis, A.Spyros and P. Dais, Polymer, 1993, 34, 1846.
1	"Structure and dynamics of poly(1-naphthyl acrylate) in solution by 13C NMR spectroscopy". A. Spyros and Photis Dais, Macromolecules, 1992, 25, 1062. (pdf)